8. 7  A Powerful Tool for X-Ray Diffraction Experiments
- Focusing Mechanism for One-Order of Magnitude Increase in the Density of Wide-Band Synchrotron X-Rays
 


Fig. 8-15 Bending mechanism for the Si crystal used in the double-crystal monochromator

At the center, the height of the crystal is maintained at any radius of bend.


Fig. 8-16 Schematic for a series of crystal slabs joined by thin hinge regions

In order to make an ideal cylindrical shape, a series of crystal slabs joined by thin hinge regions are used.


Fig. 8-17 Beam profiles of 30 keV X-rays at the sample position (focusing point) using a sagittal-focusing double-crystal monochromator

The period of the slotted crystal is 3. 0 mm. The X-ray beam focus becomes more effective as bending radius decreases.



A bending magnetic in SPring-8 provides X-rays in a wider energy range. At the bending magnet beamline, however, the photon density decreases with a distance from the source point of the magnet because of dispersion. For the experiments, X-rays must be focused on the sample position by a bender, which can efficiently collect the dispersed beam. The focusing device is called as a sagittal focusing bender.
Sagittal focusing has been required at a standard beamline of the bending magnet in Spring-8 as well. However, a ready-made bender is not available for X-rays of a wide energy range from the bending magnet in SPring-8. Thus an original bender used for an energy range of 8 - 150 keV has been developed (Fig. 8-15). The new device can bend the second Si crystal (Fig. 8-16) of a double-crystal monochromator into ideally cylindrical shape without introducing any deformation in the crystal.
Good results have been obtained in the performance test where the inclined 111, 511 and 733 reflections have enabled us to focus high energy X-rays up to 30 keV, 100 keV and 150 keV, respectively, quite efficiently (Fig. 8-17). In the whole energy range one order of magnitude increase in the photon density has been achieved without a decrease in the energy resolution. Now the new sagittal focusing benders have been installed in SPring-8 as standard monochromators. In BL14B1 (JAERI beamline), the bender is effectively used for the structure analysis of non-crystalline materials.



Reference
Y. Yoneda et al., Fixed-Height Exit Bender of Synchrotron X-Rays Above 40 keV, J. Synchrotron Rad., 8, 18 (2001).

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Persistent Quest - Research Activities 2001
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