7.2 Observe the Microscopic Fractures of Polycrystalline Ceramics

Fig. 7-4 Fracture probability distribution of the tensile strength of graphite
Predicted values were compared with experimental values. In the fine grained graphite the predicted values coincide well with the experimental ones if the pore size parameter (Sd) is taken to be large (Sd=1.9¨Sd=2.0).

Fig. 7-5 Fracture probability distribution of bending strength of silicon carbide
Predicted values were compared with experimental ones for silicon carbide materials having different grain sizes. The figure indicates that the new fracture model is roughly applicable to the bending strength.


Recently, a model illustrating the fracture mechanism taking account of microstructures of polycrystalline ceramics has been developed. It successfully illustrates the tensile and bending strengths of the ceramics. This is a probabilistic fracture strength model taking into consideration the average grain size, pore number density, average pore diameter, pore diameter distribution parameter, fracture toughness of a grain, and specimen volume. The model assumes that the material consists of a collective of cubic crystalline particles of the same size. The calculation of fracture probability is performed for the material in which slit-like cracks placed uniformly and with random slopes to the stress axis grow in the crystal grain. The six parameters described above are needed to calculate the fracture probability. The first model was applicable to the tensile strength and this model was extended to be applicable to the bending strength. Figure 7-4 shows a comparison of experimental values with the predicted ones when the model was applied to the tensile strength of graphite. Both values for the coarse grained graphite (PGX) coincide well. In the case of the fine grained graphite (IG-110) both values coincide well if the pore size parameter is taken to be large (Sd=2.0). This suggests that large size pores are dominant in the fracture of the ceramics. When the model is applied to the bending strength of silicon carbide, the result shown in the Fig. 7-5 is obtained. The experimental results indicate that the bending fracture strengths of three kinds of silicon carbide (three different grain sizes) can be well illustrated by the model.


Reference
K. Nakanishi et al., Microstructure-Based Prediction of Fracture Probability of Polycrystalline SiC, Nippon Kikai Gakkai Dai-10kai Keisanrikigaku Koenkai Koen Ronbunshu, 97 (7), 323 (1997).

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